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Polymeric Foams And Foam Technology - Klempner, Daniel (EDT)/ Sendijarevic, vahid

Polymeric Foams And Foam Technology

por Klempner, Daniel (edt) ; Sendijarevic, Vahid

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Formato: Tapa dura (Hardcover)
Editorial: Hanser Gardner Pubns
Año de Edición: 2004/04/01
Tema: TECHNOLOGY & ENGINEERING / Material Science
Tags: Plastic foams
Idioma: Inglés
Peso: 1380.16 gramos
Estado: Nuevo
ISBN: 1569903360
ISBN 13: 9781569903360
Precio: US$ 267,70
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Resumen del libro
Publisher Summary 1
Klempner (University of Detroit) and Sendijarevic (Troy Polymers, Inc.) collect material on all major classes of polymeric foams and describe their chemistry, properties, preparation methods, and applications. Fundamental aspects of foam are first explained, then specific classes are examined, including polyurethane and isocyanate-based polymeric foams, polystyrene, polyolefin, poly (vinyl chloride), and latex. A final chapter discusses blowing agents for polymer foams. This second edition reflects developments in environmentally acceptable blowing agents, combustibility, and solid waste disposal that have occurred over the past ten years, and describes new classes of foam now in use. The book is of interest to industrial and academic scientists and engineers working in polymeric foams. Annotation ©2004 Book News, Inc., Portland, OR (booknews.com)
 


Tabla de Contenidos del libro
Preface ix
1 Introduction
1(4)
1.1 References
4(1)
2 Fundamentals of Foam Formation
5(12)
2.1 Introduction
5(1)
2.2 Fundamental Principles of Foam Formation
6(5)
2.2.1 Bubble Formation
6(2)
2.2.2 Bubble Growth
8(1)
2.2.3 Bubble Stability
9(2)
2.3 Supporting Evidence from Specific Foam Systems
11(2)
2.3.1 Thermoplastic Foams
11(1)
2.3.2 Polyurethane Foams
12(1)
2.3.3 Cellular Rubber
13(1)
2.4 Summary
13(1)
2.5 References
14(3)
3 Cellular Structure and Properties of Foamed Polymers
17(38)
3.1 Introduction
17(1)
3.2 Porous and Cellular Systems
17(5)
3.2.1 Statistical Meaning of the Concept of a Cell
17(1)
3.2.2 Terminology
18(1)
3.2.3 Basic Relationships
19(1)
3.2.4 Packing Types
20(2)
3.3 Open- and Closed-Cell Foamed Plastics
22(2)
3.3.1 General Problems
22(1)
3.3.2 Open Cells and Density
23(1)
3.3.3 Reticulated Foams
24(1)
3.4 Density of Foamed Polymers
24(4)
3.4.1 Classification
24(1)
3.4.2 Density and Cell Size
25(1)
3.4.3 Density and Wall Thickness
26(2)
3.5 Cell Shape of Foamed Polymers
28(5)
3.5.1 Cell Shape Models
28(1)
3.5.2 12- and 14-Hedrons
28(2)
3.5.3 Anisotropy of Cell Shapes
30(3)
3.6 Cell Size of Foamed Polymers
33(5)
3.6.1 Methods of Estimation
33(1)
3.6.2 Cell Size and Number of Cells
34(1)
3.6.3 Cell Size and Wall Thickness
34(1)
3.6.4 Microcells
35(2)
3.6.5 Cell Size and Physical Properties
37(1)
3.7 Models of Cellular Structure and Calculation of Mechanical Properties of Foamed Polymers
38(2)
3.7.1 Flexible Foamed Polymers
38(1)
3.7.2 Rigid Foamed Polymers
39(1)
3.8 Cellular Structure and Thermal Conductivity of Foamed Polymers
40(7)
3.8.1 Thermal Conductivity of the Polymer Phase
41(1)
3.8.2 Thermal Conductivity of the Gas Phase
41(3)
3.8.3 Radiative Thermal Conductivity
44(1)
3.8.4 Convective Thermal Conductivity
45(1)
3.8.5 Effects of Variables on the Thermal Conductivity
46(1)
3.9 General Concepts
47(5)
3.9.1 Three Generations of Polymer Foams
47(1)
3.9.2 Six Structural Levels
48(1)
3.9.3 Quantitative Parameters of Cellular Structure
49(1)
3.9.4 Technological Concepts
50(1)
3.9.5 Advantages of Foamed Polymers
51(1)
3.10 References
52(3)
4 Flexible Polyurethane Foams
55(66)
4.1 introduction
55(2)
4.1.1 Applications
55(1)
4.1.2 Markets
56(1)
4.2 Basic Chemistry
57(20)
4.2.1 The Polymerization Reaction
59(1)
4.2.2 The Gas-Producing Reaction
60(1)
4.2.3 Foam Recipe Components
61(16)
4.3 Foam Morphology
77(7)
4.3.1 Review of Current Concepts
77(7)
4.3.2 Model for Flexible Foam Formation
84(1)
4.4 Preparation of Flexible Foam
84(10)
4.4.1 General Requirements
85(1)
4.4.2 Laboratory-Scale Cup-Foaming
86(1)
4.4.3 Laboratory Box-Foams
86(1)
4.4.4 Machine-Made Foam
87(1)
4.4.5 Mixing Heads
88(1)
4.4.6 Commercial-Scale Processes
89(5)
4.5 Foam Physical Properties
94(6)
4.5.1 Foam Density
95(1)
4.5.2 Load Bearing
95(2)
4.5.3 Airflow
97(1)
4.5.4 Cell Size
97(1)
4.5.5 Compression Set
98(1)
4.5.6 Tension Properties
99(1)
4.5.7 Tear
99(1)
4.5.8 Resilience
100(1)
4.6 Slabstock Foams
100(5)
4.6.1 Slabstock Chemistry
100(1)
4.6.2 Alternative Blowing Agent Developments
100(1)
4.6.3 High Load Bearing Foams
101(1)
4.6.4 High Resilience Foams
102(1)
4.6.5 Foam Flammability
102(1)
4.6.6 Non-BHT Foams
103(1)
4.6.7 Emanations
104(1)
4.6.8 Recycling
104(1)
4.7 Molded Foam
105(4)
4.7.1 Seating Foams
105(1)
4.7.2 Comfort
106(1)
4.7.3 Durability
107(1)
4.7.4 Fogging and Odor
108(1)
4.8 References
109(12)
5 Rigid Polyurethane Foams
121(20)
5.1 Introduction
121(1)
5.2 Structure
122(1)
5.3 Chemistry
122(1)
5.4 Reactants
123(4)
5.4.1 Isocyanates
123(1)
5.4.2 Polyols
124(1)
5.4.3 Catalysts
125(1)
5.4.4 Stabilizers
126(1)
5.4.5 Blowing Agents
126(1)
5.4.6 Combustion Modifiers
127(1)
5.5 Formulations
127(1)
5.6 Foam Preparation
128(2)
5.6.1 Block and Sheet
129(1)
5.6.2 Pour-in-Place
129(1)
5.6.3 Spray
130(1)
5.7 Foam Physics
130(1)
5.8 Properties
131(5)
5.8.1 Density
131(1)
5.8.2 Mechanical Properties
131(1)
5.8.3 Water, Solvent, and Chemical Resistance
132(1)
5.8.4 Thermal Conductivity
132(2)
5.8.5 Combustibility
134(2)
5.9 Applications
136(1)
5.10 Health and Safety
136(1)
5.10.1 Isocyanates
137(1)
5.10.2 Polyols
137(1)
5.10.3 Catalysts
137(1)
5.10.4 Blowing Agents
137(1)
5.11 Future Trends
138(1)
5.12 References
138(2)
Acknowledgement
140(1)
6 Polyisocyanurate Foams
141(48)
6.1 Introduction
141(2)
6.2 Isocyanurate Chemistry
143(17)
6.2.1 Catalysts for Cyclotrimerization
143(5)
6.2.2 Kinetics and Mechanisms of Cyclotrimerization
148(8)
6.2.3 Relative Catalytic Activity
156(4)
6.3 Preparation of Modified Polyisocyanurate Foams
160(20)
6.3.1 Urethane-Modified Polyisocyanurate Foams
160(15)
6.3.2 Oxazolidone-Modified Polyisocyanurate Foams
175(3)
6.3.3 Amide-Modified Polyisocyanurate Foams
178(1)
6.3.4 Carbodiimide-Modified Polyisocyanurate Foams
178(1)
6.3.5 Imide-Modified Polyisocyanurate Foams
179(1)
6.4 Applications
180(4)
6.4.1 Composite Foam Boards
180(1)
6.4.2 Flame-Retardant Seamless Insulation [61]
181(1)
6.4.3 Building Insulation
182(1)
6.4.4 Chemical and Petrochemical Plant Insulation
183(1)
6.4.5 High-Rise Building Walls
183(1)
6.4.6 Chemical-Resistant Floats
183(1)
6.4.7 Cryogenic, Petrochemical, and Solar Energy Applications
183(1)
6.4.8 Highly Resilient Flexible Polyurethane Foams
184(1)
6.5 References
184(5)
7 Polystyrene and Structural Foam
189(44)
7.1 Introduction and General Description
189(1)
7.1.1 Nomenclature
190(1)
7.2 Chemistry and Preparation
190(5)
7.2.1 Theory of the Expansion Process
191(2)
7.2.2 Blowing Agent Selection
193(2)
7.3 Properties and Their Relation to Structure
195(13)
7.3.1 Test Methods
195(1)
7.3.2 Properties of Commercial Products
195(4)
7.3.3 Mechanical Properties
199(5)
7.3.4 Thermal Properties
204(2)
7.3.5 Moisture Resistance
206(1)
7.3.6 Electrical Properties
207(1)
7.3.7 Environmental Aging
207(1)
7.3.8 Other Properties
207(1)
7.4 Commercial Production and Processing
208(6)
7.4.1 Manufacturing Process
208(4)
7.4.2 Commercial Products and Processes
212(2)
7.5 Applications
214(11)
7.5.1 Cushioning
215(1)
7.5.2 Thermal Insulation
216(1)
7.5.3 Packaging
217(2)
7.5.4 Structural Components
219(1)
7.5.5 Marine Applications
219(1)
7.5.6 Electrical Insulation
219(1)
7.5.7 Space Filling and Seals
219(1)
7.5.8 Other Uses
220(1)
7.5.9 Energy Considerations in Foam Insulation
220(4)
7.5.10 Health and Safety Factors
224(1)
7.6 References
225(8)
8 Polyolefin Foam
233(68)
8.1 Introduction
233(1)
8.2 Chemistry and Preparation
234(28)
8.2.1 Foam Expansion with a Physical Blowing Agent
237(11)
8.2.2 Foam Expansion with a Chemical Blowing Agent
248(14)
8.3 Properties and Their Relation to Structure
262(13)
8.3.1 Properties of Commercial Products
266(1)
8.3.2 Relationships Between Structure and Properties
267(8)
8.4 Commercial Production and Processing
275(13)
8.4.1 Extrusion Processes
275(3)
8.4.2 Processes for Manufacturing Moldable Polyolefin Beads
278(3)
8.4.3 Cross-Linked Polyolefin Foam Sheet Processes
281(5)
8.4.4 Cross-Linked Polyolefin Foam Bun Stock Processes
286(2)
8.5 Applications
288(5)
8.5.1 Fabrication
288(1)
8.5.2 Major Applications
289(4)
8.6 References
293(8)
9 PVC Foams
301(46)
9.1 Introduction
301(2)
9.2 Characteristics of PVC
303(2)
9.2.1 PVC Structures
304(1)
9.2.2 Structure Changes During Processing
305(1)
9.2.3 Influence of PVC Fusion on Physical Properties
305(1)
9.3 Formulation Technology
305(15)
9.3.1 Overview of Formulas for PVC Foam
305(3)
9.3.2 Effects of Formulation Ingredients on the Foaming Process and Properties of Foamed Products
308(9)
9.3.3 Use of Recycled PVC in Foam Formulations
317(1)
9.3.4 Design of Experiment (DOE) for Foam Formulation Development
318(2)
9.4 Processing Technology
320(15)
9.4.1 Extrusion of PVC Foams
321(7)
9.4.2 Injection Molding of PVC Foams
328(1)
9.4.3 Foaming of PVC at Atmospheric Pressure
329(2)
9.4.4 Microcellular PVC Foams
331(3)
9.4.5 PVC/Wood Flour Composite Foams
334(1)
9.5 Mechanical Property Analyses and Test Standards
335(6)
9.5.1 Mechanical Properties
336(4)
9.5.2 ASTM and ISO Standards
340(1)
9.6 References
341(6)
10 Epoxy Foams 347(20)
10.1 Introduction
347(1)
10.2 Epoxy Chemistry and Formulations
347(2)
10.3 Blowing or Foaming Agents and Processes
349(1)
10.3.1 Inert Gas Blowing Agents
350(1)
10.3.2 Inert Liquid Blowing Agents
350(1)
10.3.3 Reactive Blowing Agents
350(1)
10.3.4 Expanding Syntactic Fillers
351(1)
10.3.5 Frothed Epoxies
352(1)
10.3.6 Epoxy Emulsions
352(1)
10.3.7 Non-Aqueous Liquid Extractable Pore Formers and CIPS
352(1)
10.3.8 Solid Extractable Pore Formers
353(1)
10.3.9 Stereolithography
353(1)
10.4 Combinations of Epoxy and Isocyanate Based Thermosets
354(1)
10.5 Three-Phase Syntactics
355(1)
10.6 Fiber-Reinforced Foams
356(1)
10.7 Removable Foams
356(1)
10.8 Applications
357(1)
10.8.1 Automotive (also See Adhesive Applications Below)
357(1)
10.8.2 Electronics Encapsulation
359(1)
10.8.3 Adhesives
361(1)
10.8.4 Building Retrofitting
361(1)
10.8.5 Dams, Tanks and Bridges
362(1)
10.8.6 Expanding Cores
362(1)
10.8.7 Sports Equipment
362(1)
10.8.8 Personal Care Products
363(1)
10.8.9 Thermoplastic Processing and Recycling
363(1)
10.8.10 Lung Substitutes
363(1)
10.9 References
363(4)
11 Latex Foam and Sponge 367(12)
11.1 Introduction
367(2)
11.2 Dunlop Process
369(1)
11.2.1 Compounding Ingredients
369(1)
11.2.2 Processing Notes
370(1)
11.2.3 Foaming
371(2)
11.3 Freeze Process
373(1)
11.3.1 Original Freeze Process
374(1)
11.3.2 Newer Freeze Process
374(1)
11.4 Sponge
374(1)
11.4.1 Open-Cell Sponge Rubber
374(1)
11.4.2 Closed-Cell Sponge Rubber
375(3)
11.5 References
378(1)
12 Silicone Foams 379(12)
12.1 Background and Development
379(1)
12.1.1 Background
379(1)
12.1.2 Development of Silicone Foams
379(1)
12.1.3 Development of Flame-Retardant Foam Technology
381(1)
12.2 Chemistry and Preparation
381(1)
12.2.1 Foam Formation
381(1)
12.2.2 Optional ingredients
381(1)
12.2.3 Preparation
384(1)
12.3 Properties and Their Relationship to Structure
384(1)
12.3.1 Structural Features
384(1)
12.3.2 Physical Properties
384(2)
12.4 Commercial Production and Processing
386(1)
12.4.1 Metering
386(1)
12.4.2 Mixing
386(1)
12.4.3 Dispensing
387(1)
12.4.4 Equipment Selection
388(1)
12.5 Applications
388(1)
12.5.1 Foam Applications
388(1)
12.5.2 Forms of Foam
388(1)
12.5.3 Features of Silicone Products
388(1)
12.5.4 Areas of Application
389(1)
12.6 References
389(2)
13 Fluoropolymer Foams 391(18)
13.1 History and Introduction
391(1)
13.2 Chemistry and Physics of Foam Preparation
392(1)
13.2.1 Nucleation and Bubble Growth
393(4)
13.3 Properties and Their Relation to Cell Structure
397(1)
13.3.1 Physical Properties
397(1)
13.3.2 Thermal Properties
399(1)
13.3.3 Specific Heat
400(1)
13.3.4 Electrical Properties
400(2)
13.4 Commercial Production and Processing
402(1)
13.4.1 Foaming of FEP and PFA Resins
402(1)
13.4.2 Foaming of Fluoroelastomer Resins (such as Viton)
403(1)
13.4.3 Expansion of PTFE Resin
404(1)
13.5 Applications
405(1)
13.6 References
406(3)
14 Wood Flour Composite Foams 409(38)
14.1 Introduction
409(1)
14.1.1 Background on Polymeric Composites
409(1)
14.1.2 Natural Fibers and Their Properties
410(1)
14.1.3 Plastic/Wood Flour Composite Foams
413(2)
14.2 Major Issues in Development of PWC Foams
415(1)
14.2.1 Thermal Degradation of Natural Fibers
416(1)
14.2.2 Moisture Content and Volatile Emissions from Natural Fibers
418(1)
14.2.3 Dispersion of Natural Fiber and Fiber-Matrix Bonding
420(1)
14.2.4 Processing Difficulties Due to Increased Viscosity
420(1)
14.3 Phase Changes in Foaming of PWC
421(1)
14.3.1 Changes in Phase Morphology of the Extrudate During Microcellular Foaming and Fine-Celled PWC Foaming
421(1)
14.3.2 Polymer/Gas Solution Formation
422(1)
14.3.3 Cell Nucleation
423(1)
14.3.4 Cell Growth Control
424(2)
14.4 Experiments and Discussion
426(1)
14.4.1 Effects of Volatile Emissions from Wood Flour During Extrusion Processing
427(1)
14.4.2 Foaming Experiments with Varying Content of Extractives
431(1)
14.4.3 Critical Processing Temperature in Extrusion Processing of PWC Foams
434(1)
14.4.4 Foaming with Various CBAs
439(3)
14.5 Conclusions
442(1)
14.6 References
443(4)
15 Phenolic Foams 447(10)
15.1 Chemistry and Foam Formation
447(1)
15.1.1 Phenolic Resins
447(1)
15.1.2 Crosslinking of Phenolic Resins
449(1)
15.1.3 Foam Formation
450(1)
15.1.4 Reduction in Corrosivity of Phenolic Foam
452(1)
15.2 Properties and Their Relation to Structure
452(2)
15.3 Commercial Production and Processing
454(1)
15.4 Applications
455(1)
15.5 References
455(2)
16 Flame Retardancy of Polymeric Foams 457(22)
16.1 Introduction
457(1)
16.2 The Combustion of Polymeric Foams
458(1)
16.2.1 Flame Combustion of Polymeric Foams
458(1)
16.2.2 Smoldering Combustion of Polymeric Foams
460(1)
16.2.3 Filtration Combustion of Gases in Polymeric Foams
462(1)
16.3 Test Methods and Fire Safety Classification Parameters
463(1)
of Foamed Materials for the Assessment of Fire Hazards
463(5)
16.4 Recent Advances in Flame Retardancy of Polymeric Foams
468(1)
16.4.1 The Development of Foams Based on Inherently Thermally Stable and Flame Retardant Polymers
468(1)
16.4.2 Chemical and Physical Modification of Polymeric Foams
470(1)
16.4.3 Additive Flame Retardants
471(1)
16.5 References
475(4)
17 Syntactic Polymer Foams 479(26)
17.1 Introduction
479(1)
17.2 Hollow Sphere Fillers
480(1)
17.2.1 General Information
480(1)
17.2.2 Glass Microspheres
480(1)
17.2.3 Polymeric Micro spheres
481(1)
17.2.4 Miscellaneous Other Microspheres
482(1)
17.2.5 Macrospheres
482(1)
17.3 Syntactic Foam Processing
482(1)
17.3.1 General Considerations
482(1)
17.3.2 Rheology of Syntactic Mixtures
483(1)
17.3.3 Casting and Molding Compositions
483(1)
17.3.4 Regulating the Apparent Density
484(1)
17.3.5 Microsphere Space Factors and Packing
485(2)
17.4 Syntactic Foam Production
487(1)
17.4.1 Epoxy Syntactic Foams
487(1)
17.4.2 Oligoester Syntactic Foams
488(1)
17.4.3 Phenolic Syntactic Foams
488(1)
17.4.4 Organosilicone Syntactic Foams
489(1)
17.4.5 Polyimide Syntactic Foams
489(1)
17.4.6 Carbonized Syntactic Foams
489(1)
17.4.7 Syntactic Prepregs
490(1)
17.4.8 Miscellaneous Syntactic Foams
491(1)
17.5 Physical Properties of Syntactic Foams
491(1)
17.5.1 Strength Properties
491(1)
17.5.2 Water Absorption and Resistance to Hydrostatic Pressure
494(1)
17.5.3 Thermal Properties
496(1)
17.6 Recent Developments and Main Applications
497(1)
17.6.1 Sub-Sea and Shipbuilding Applications
497(1)
17.6.2 Structural Applications
500(1)
17.6.3 Aerospace Applications
502(1)
17.6.4 Other Applications
503(1)
17.7 References
503(2)
18 Blowing Agents for Polymeric Foams 505(44)
18.1 Introduction
505(1)
18.2 Classification
505(2)
18.3 Chemical Blowing Agents
507(1)
18.3.1 Main Characteristics
507(1)
18.3.2 Inorganic Blowing Agents
509(1)
18.3.3 Organic Blowing Agents
511(1)
18.3.4 Blowing Agents that Liberate Gases as a Result of Chemical Interaction between the Components
532(1)
18.3.5 Practical Guide for Selection of CBAs
536(3)
18.4 Physical Blowing Agents and Environmental Problems
539(1)
18.4.1 Main Characteristics
539(1)
18.4.2 Volatile Liquids
540(1)
18.4.3 Solid Blowing Agents
546(1)
18.5 Gases
546(1)
18.6 Nucleazites
546(1)
18.7 References
547(2)
Appendix 1 549(3)
Letters of the Roman Alphabet
549(1)
Capital Greek Letters
550(1)
Lower Case Greek Letters
551(1)
Appendix 2 Conversion Factors between English and S.I. Units for Quantities 552
Used in Describing the Physical Properties of Foams
552


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